Adelaide Research & Scholarship
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https://hdl.handle.net/2440/124924
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| Type: | Journal article |
| Title: | Synthesis of per-deuterated alkyl amines for the preparation of deuterated organic pyromellitamide gelators |
| Author: | Yepuri, N. Jamieson, S. Darwish, T. Rawal, A. Hook, J. Thordarson, P. Holden, P. James, M. |
| Citation: | Tetrahedron Letters: the international journal for the rapid publication of all preliminary communications in organic chemistry, 2013; 54(20):2538-2541 |
| Publisher: | Elsevier |
| Issue Date: | 2013 |
| ISSN: | 0040-4039 1873-3581 |
| Statement of Responsibility: | Nageshwar R.Yepuri, Scott A.Jamieson, Tamim A.Darwish, Aditya Rawal, James M.Hook ... Michael James ... et al. |
| Abstract: | A general, direct and scalable synthesis of per-deuterated alkyl amines is reported, together with their incorporation into pyromellitamides, which form self-assembled gels in cyclohexane. The deuterium labelling of these gelators allows the study of the dynamic intermolecular interactions in these materials using solid-state 2H NMR spectroscopy. |
| Keywords: | Self-assembling organogels; deuterated amines; supramolecular chemistry; solid state deuterium NMR |
| Rights: | © 2013 Published by Elsevier Ltd. All rights reserved. |
| DOI: | 10.1016/j.tetlet.2013.03.031 |
| Grant ID: | http://purl.org/au-research/grants/arc/DP09855059 http://purl.org/au-research/grants/arc/FT120100101 |
| Published version: | http://dx.doi.org/10.1016/j.tetlet.2013.03.031 |
| Appears in Collections: | Aurora harvest 4 Chemistry publications |
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