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https://hdl.handle.net/2440/27356
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dc.contributor.author | Stevens, D. | - |
dc.contributor.author | McLaughlin, M. | - |
dc.contributor.author | Alston, A. | - |
dc.date.issued | 1995 | - |
dc.identifier.citation | Communications in Soil Science and Plant Analysis, 1995; 26(11-12):1823-1842 | - |
dc.identifier.issn | 0010-3624 | - |
dc.identifier.issn | 1532-2416 | - |
dc.identifier.uri | http://hdl.handle.net/2440/27356 | - |
dc.description.abstract | Procedures for determination of fluoride (F) in plant material employing acid digestion and solution analysis by ion specific electrode (ISE) were compared to alkali fusion using a range of plant materials. The efficiency of the methods were assessed using standard reference plant material (SRM) not previously available for plant F analysis. All acid digestion procedures tested failed to obtain the certified value for F in the SRM. This was due to failure of the acids to liberate F bound strongly within silicate minerals found in the plant materials. Acid digestion is therefore not recommended for determination of total F, but could be used to determine labile F in plant materials. During investigation of the acid digestion procedures, it was also found that F concentrations determined in solution using the ISE are sensitive to solution pH, even at solution pH values where complexation of F with hydrogen ions (H⁺) can be discounted. It is therefore recommended that both ionic strength and pH of sample and standard solutions be matched when determining F concentrations in solution using the F-ISE. | - |
dc.language.iso | en | - |
dc.publisher | M. Dekker | - |
dc.source.uri | http://dx.doi.org/10.1080/00103629509369411 | - |
dc.subject | Plant tissue | - |
dc.subject | Assay | - |
dc.subject | Fluorides | - |
dc.subject | Sample preparation | - |
dc.subject | Acid digestion | - |
dc.subject | Microwave | - |
dc.subject | Ion selective electrode | - |
dc.subject | Analysis method | - |
dc.subject | Inorganic element | - |
dc.title | Limitations of acid digestion techniques for the determination of fluoride in plant material | - |
dc.type | Journal article | - |
dc.identifier.doi | 10.1080/00103629509369411 | - |
pubs.publication-status | Published | - |
dc.identifier.orcid | McLaughlin, M. [0000-0001-6796-4144] | - |
Appears in Collections: | Aurora harvest 2 Environment Institute publications Soil and Land Systems publications |
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