Adelaide Research & Scholarship
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https://hdl.handle.net/2440/57161
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| Type: | Journal article |
| Title: | Synthesis of macrocyclic β-Strand memplates by ring closing metathesis |
| Other Titles: | Synthesis of macrocyclic beta-Strand memplates by ring closing metathesis |
| Author: | Abell, A. Alexander, N. Aitken, S. Chen, H. Coxon, J. Jones, M. McNabb, S. Muscroft-Taylor, A. |
| Citation: | Journal of Organic Chemistry, 2009; 74(11):4354-4356 |
| Publisher: | Amer Chemical Soc |
| Issue Date: | 2009 |
| ISSN: | 0022-3263 1520-6904 |
| Statement of Responsibility: | Andrew D. Abell, Nathan A. Alexander, Steven G. Aitken, Hongyuan Chen, James M. Coxon, Matthew A. Jones, Stephen B. McNabb and Andrew Muscroft-Taylor |
| Abstract: | We report the synthesis of macrocycles 1-6 via ring closing metathesis of dienes 7-12. Addition of chlorodicyclohexylborane to thermal and microwave assisted RCM of dienes 8 and 9 markedly improves the yield. The geometric isomers of macrocycles 1-3 and 5 have been assigned using X-ray crystallography and NMR. |
| Rights: | © 2009 American Chemical Society |
| DOI: | 10.1021/jo802723w |
| Grant ID: | ARC |
| Published version: | http://dx.doi.org/10.1021/jo802723w |
| Appears in Collections: | Aurora harvest Chemistry publications |
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