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https://hdl.handle.net/2440/85923
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Type: | Journal article |
Title: | Determination of oxalate in alumina process liquors by ion chromatography with post column chemiluminescence detection |
Author: | Barnett, N.W. Bowser, T.A. Russell, R.A. |
Citation: | Analytical Proceedings, 1995; 32(2):57-59 |
Publisher: | Royal Society of Chemistry |
Issue Date: | 1995 |
ISSN: | 0144-557X |
Statement of Responsibility: | Neil W. Barnett, Tim A. Bowser and Richard A. Russell |
Abstract: | The analysis of oxalate in Bayer liquor had been successfully demonstrated using a combination of ion-exchange chromatography and post-column detection based on a chemiluminescence reaction with tris(2-2′bipyridyl)ruthenium(III). Common interferences, including other dicarboxylic acids and inorganic anions, have been shown to elicit no significant response. The chemiluminescence response is linear and a detection limit of 10–7 mol l–1 possible. The potential use of this method for other complex samples is presented. Chromatographic conditions provide a rapid analysis with sample analysis possible every 5–8 min. |
Rights: | Copyright status unknown |
DOI: | 10.1039/AI9953200057 |
Published version: | http://dx.doi.org/10.1039/ai9953200057 |
Appears in Collections: | Aurora harvest 7 Chemistry publications |
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